To have passed the exams of General and Inorganic Chemistry with Laboratory, Analytical Chemistry I with Laboratory and Analytical Chemistry II with Laboratory
Three mid-term assessments, multiple-choice and open questions exams, whose results will be communicate to the Student before the final exam.
Final oral exam
Critical discussion on written reports on laboratory experiences.
The final vote will take account of the three tests.
The aim of the course is to provide to the Student the necessary competences of instrumetal chemical analysis with chromatographic and spectroscopic (IR) techniques. At the end of the course the Student will acquire theoretical and practical knowledge about the chromatographic separations' techniques: he will know the mechanisms of separation and concomitant phenomena, the different chromatographic techniques, instrumentation and accessories, as well as interventions to optimize the analysis. The Student will acquire similar skills on the applicability of infrared spectroscopy in quantitative analysis.
-Chromatographic separations' mechanisms
-Classification of the chromatographic techniques
-Definition and illustration of the qualitative parameters of a chromatographic separation
-Gaschromatography and HPLC: kind of phases, classification and detailed description of the tecniques, instrumentation and practical applications
-Infrared spectroscopy: theory, instrumentation and applications in quantitative analysis.
Cozzi, Protti, Ruaro, Elementi di analisi chimica strumentale, Zanichelli Editore, (chapters 9, 12, 14, 15, 16)
Slides and supplementary lecture notes.
Lectures (64 hours) and Labs (32 hours). Lectures with the aid of supplementary material to the textbooks (slides), description of equipment and accessories in the laboratory, quantitative analysis of different analytes in real samples, after calibration, through the techniques described in the course.
The integrative material used during the course will be shared with the Students.
1) Readiness to offer individual assistance also in English language to incoming students through appointment fixed by e-mail (email@example.com)
2) Availability of supporting material and bibliographic references also in english language.
List: David Hardey, Modern Analytical Chemistry, McGraw-Hill
3) Readiness to accept examination of incoming students also in a foreign language (English)
4) As estabilished in the document "Manifesto degli Studi", the course attendance is mandatory (https://www.dcf.uniss.it/it/didattica/corsi-di-studio/chimica)