ORGANIC QUALITATIVE PHARMACEUTICAL CHEMICAL ANALYSIS

Single discipline educational activity

Course Sheet

Academic Year of enrolment:

2018/2019

Type of Course:

Characterising

Optional/Mandatory:

Compulsory

Degree:

5-year Single Cycle Master's Degree Programme in PHARMACEUTICAL CHEMISTRY AND TECHNOLOGY

Disciplinary Sector:

Pharmaceutical Chemistry

Language:

Italian

Credits:

Programme Year:

Professor and Collaborators:

PIRAS Sandra

Obligatory attendance:

Yes

Hours of classroom activity:

102

Prerequisites:

To attend the course is recommended, while to support the exam is compulsory, the students have to supported the exams: general chemistry, organic chemistry, advanced organic chemistry, Chemical pharmaceutical analisys

AF code:

40000822

Assessment Methods

Verification of learning:

Final oral exam

Teaching period

Second semester

Objectives

The aim of the course is to provide knowledges, practice expertises and metodology to identify drugs of European Pharmacopeia

Contents

The course provides a systematic approach to the identification of an unknown substance, based on the chemical behavior of the compound, through selective chemical assays for the identification of the main functional groups and specific assays present in the Pharmacopoeia. Combustion, Qualitative Elemental Analysis (Lassaigne), Le Rosen and Friedl-Craft, oxidation reactions, reaction of iodoform.Solubility. Functional group reactions. Identification of medicines recorded in the European Pharmacopeia 7th Edition.

Recommended Bibliography

1) A. Carta, M. G. Mamolo, F. Novelli, S. Piras: "Analisi Farmaceutica Qualitativa". Edises
3) Farmacopea Europea.
4) H.J.Roth, K.Eger, R.Troschutz:”Pharmaceutical chemistry. Volume II. Drug analysis”. Ellis Horwood, New York.

Methods of Provision

Conventional

Teaching Methods

40 hours face to face.individual laboratory exercises :70 hours.

Contacts/More Information

1) Readiness to offer individual assistance also in English language to incoming students
2) Availability of supporting material and bibliographic references also in english language.
List:H.J.Roth, K.Eger, R.Troschutz:”Pharmaceutical chemistry. Volume II.
Drug analysis”. Ellis Horwood, New York.

3) Readiness to accept examination of incoming students also in a foreign language (English)

ORGANIC QUALITATIVE PHARMACEUTICAL CHEMICAL ANALYSIS

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ORGANIC QUALITATIVE PHARMACEUTICAL CHEMICAL ANALYSIS