MS-INTERFACE SYSTEMS IN THE INSTRUMENTAL CHEMICAL ANALYSIS

Single discipline educational activity

Course Sheet

Academic Year of enrolment:

2013/2014

Type of Course:

Elective Course

Optional/Mandatory:

Optional

Degree:

Master's Degree Programme in CHEMICAL SCIENCES

Disciplinary Sector:

Analytical Chemistry

Language:

Italian

Credits:

Programme Year:

Professor and Collaborators:

SANNA Gavino

Hours of classroom activity:

Prerequisites:

No prerequisites

AF code:

40004013

Assessment Methods

Verification of learning:

The exam will be held in oral or written form.

Teaching period

Second semester

Objectives

The course aims to provide an updated overview on the characteristics and capabilities of chromatographic (or spectroscopic) instruments hyphenated with a mass spectrometer. Another key point of the course is the definition and evaluation of the most meaningful validation parameters of an analytical method.

Contents

The mass spectrometer (MS). Ionization systems and sample introduction devices. Analyzers and thei resolution. Detectors. Supercritical Phase Chromatograpy (SPC). Capillary Electrophoresis (CE), Inductively Coupled Plasma spectroscopy (ICP). MS-MS, GC-MS, LC-MS, SPC-MS, CE-MS, ICP-MS couplings. Outlines of the procedure for the validation of analytical method.

Recommended Bibliography

R. Kellner, J.-M. Mermet, M. Otto, H.M. Widmar, Chimica Analitica, EdiSES, 2003
Cozzi-Protti-Ruaro: Analisi Chimica Strumentale. Seconda Edizione, Volumi 1, 2 e 3, Zanichelli, 1997
Skoog-Leary: Chimica Analitica Strumentale, EdiSES, 1995
Power point presentations used in the face-to-face lessons
Papers and reviews (in english language)

Methods of Provision

Conventional

Teaching Methods

Numerical exercises on the evaluation of selected validation parameters

Contacts/More Information

1) Readiness to offer individual assistance also in English language to incoming students
2) Availability of supporting material and bibliographic references also in english language.
List:R. Kellner, J.-M. Mermet, M. Otto, H.M. Widmar, Analytical Chemistry, Wiley-VCH: Weinheim, 1998.
D.A. Skoog and J.J. Leary. Principles of Instrumental Analysis. 4th Edition. Saunders College Publishing, Philadelphia, PA, 1992
Selected papers and reviews (in english language)

3) Readiness to accept examination of incoming students also in a foreign language (English)

Other courses

Course year: 1

CHIMICA ORGANICA SUPERIORE
8 credits - Caratterizzante
ELECTROANALYTICAL CHEMISTRY
8 credits - Caratterizzante
INORGANIC CHEMISTRY
8 credits - Caratterizzante
PHYSICAL CHEMISTRY
8 credits - Caratterizzante
POLLUTION CHEMISTRY
6 credits - Caratterizzante
SPECTROSCOPY AND STRUCTURAL CHEMISTRY
6 credits - Caratterizzante
BIO INORGANIC CHEMISTRY
6 credits - Affine/Integrativa
INNOVATIVE MATERIALS FOR ENERGY
6 credits - Affine/Integrativa
METHODOLOGIES IN INORGANIC CHEMISTRY
6 credits - Affine/Integrativa
PHARMACEUTICAL CHEMISTRY
6 credits - Affine/Integrativa
PHYSICAL METHODS IN ORGANIC CHEMISTRY
6 credits - Affine/Integrativa
MS-INTERFACE SYSTEMS IN THE INSTRUMENTAL CHEMICAL ANALYSIS
4 credits - A scelta dello studente

Course year: 2

FINAL TEST
40 credits
INDUSTRIAL AND POLYMER CHEMISTRY (ADVANCED COURSE)
8 credits - Caratterizzante
INTRODUCTION TO MATERIALS SCIENCE AND TO NANOMATERIALS CHEMISTRY
6 credits - Affine/Integrativa
ORGANIC SYNTHESIS AND LOW ENVIRONMENTAL IMPACT TECHNIQUES
6 credits - Affine/Integrativa
THEORETICAL CHEMISTRY
6 credits - Affine/Integrativa
TRAINING
2 credits - Altro

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MS-INTERFACE SYSTEMS IN THE INSTRUMENTAL CHEMICAL ANALYSIS